Simple tests comprise of a preliminary examination, density, melting point and behavior on heating. The tests must be performed in the order shown; if the density value is high, for instance, more than 1.7 gcm3 (SG greater than 1.7), then the material could well be a fluoropolymer, and heating tests must not be performed due to the danger from the fumes released.
In any heating test, only a small amount of sample should be used for the same reason, and the use of a fume cupboard is advised.
In most cases, a material’s absolute density is not needed; an approximate value is what is needed. This may be obtained by seeing if the material swims or sinks in a limited range of liquids. These may include saturated magnesium chloride and water; the former
The material, or component, has to be examined for color, transparency, its resistance to cutting, method of manufacture, etc. This is because, for example, such an examination can provide a strong hint as to the type of material used to create a particular component. A component’s weight and dimensions must also be taken into consideration, along with any flash lines, ejection marks etc.has a density of 1.34 gcm3 and the latter has a density of 1 gcm3 (When the density units are measured in gcm3 then, the value is the same as the specific gravity value.)
If the material is filled, then the density will usually be higher than that of the unfilled material, because a lot of inorganic fillers the most common fillers possess a relatively high density. The inorganic filler content can be easily estimated if a weighed sample of the material is completely burnt.
Here, a very accurate value is often not needed. The most basic method to obtain an estimated value is by heating a small sample of the material on a metal hot plate and determining the rise in temperature as well as the temperature of the hot plate just below the plastics material. It is recommended to use a heating rate of approximately 50 °C/hour, or 90 °F/hour.
An amorphous, thermoplastics material does not have a sharp melting point, while a semicrystalline, thermoplastics material typically has a sharp melting point. A glass rod is useful to move or prod the sample during heating.
Behavior on heating
During heating, thermoplastics soften while thermosetting plastics (thermosets) do not -they decompose when the temperature reaches a certain point. An amorphous, thermoplastics material will soften over a broader temperature range compared to a semi-crystalline, thermoplastics material; these have sharp melting points. This test may be often be combined with the earlier one
This information has been sourced, reviewed and adapted from materials provided by Dynisco.
38 Forge Parkway,
Franklin MA 02038
+1 508 541 9400
Pfaffenstr. 21, 74078,
+49 7131 297 0
Bldg. 7A, No. 568, Longpan Rd.
Malu, Jiading, 201801, China
+86 21 34074072-888
Lot 3615, Jalan SM 6/8
32040 Seri Manjung, Perak, Malaysia